Residue Testing

Order of the National Green Tribunal regarding sewage entering the rivers Senki, Pachin and Dikrong in Arunachal Pradesh, 08/04/2025

Order of the National Green Tribunal (Eastern Zone Bench, Kolkata) in the matter of S D Loda Vs Union of India & Others dated 08/04/2025. The state of Arunachal Pradesh and Itanagar Municipal Corporation was directed by the NGT, April 8, 2025 to file their counter affidavits on the setting …

Analysis of erythromycin and oleandomycin residues in food by high-performance liquid chromatography with fluorometric detection

A reliable and sensitive procedure is presented for the analysis of erythromycin (ERY) and oleandomycin (OLE) in food of animal origin, such as meat, liver, kidney, raw milk and egg. The method is based on a solid-phase extraction clean-up with a cation exchange cartridge, a 9-fluoromethylchloroformate (FMOC) precolumn derivatization and …

Accumulation of organochlorine pesticides and polychlorinated biphenyls in sediments, aquatic organisms, birds, bird eggs

Concentrations of polychlorinated biphenyls (PCBs), DDT and its metabolites (DDTs), HCH isomers (HCHs), chlordane compounds (CHLs) and hexachlorobenzene (HCB) were determined in sediment, soil, whole body homogenates of resident and migratory birds and their prey items (including fish, green mussel, snail, earthworm, crabs, prawn, lizard and frogs), bird eggs and …

Determination of tilmicosin residues in chicken, cattle, swine, and sheep tissues by liquid chromatography

A method was developed and validated for determination and quantitation of tilmicosin residues in swine, cattle, and sheep edible tissues, as well as chicken fat, skin, and muscle over a concentration range of 0.025 microg/g-20 microg/g. For chicken kidney and liver, the method was validated over a range of 0.060 …

Determination of streptomycin residues in food by solid-phase extraction and liquid chromatography

A reliable and sensitive procedure is presented for the analysis of streptomycin (STP) in food of animal origin, like meat, milk and honey. The method is based on a separation by ion-pair liquid chromatography with ?-naphthoquinone-4-sulfonate (NQS) postderivatization and fluorescence detection. The clean-up of the extract is done by solid-phase …

Quantitative determination of the macrolide antibiotics erythromycin, roxithromycin, azithromycin and clarithromycin

A validated, highly sensitive and precise high-performance liquid chromatographic (HPLC) method for the determination of the macrolides erythromycin, azithromycin, clarithromycin and roxithromycin in human serum is described. A diethyl ether extract, obtained from serum using a saturated sodium carbonate solution, was treated with 9-fluorenylmethyloxycarbonyl chloride (FMOC

Accumulation Features of Polychlorinated Biphenyls and Organochlorine Pesticide in Resident and Migratory Birds from South India

Persistent organochlorines such as DDT and its metabolites (DDTs), hexachlorocyclohexane isomers (HCHs), chlordane compounds (CHLs), hexachlorobenzene (HCB), and polychlorinated biphenyls (PCBs) were determined in whole-body homogenates of resident and migratory birds collected from South India. Organochlorine contamination pattern in birds varied depending on their migratory behaviour. Resident birds contained relatively …

Analysis of macrolide antibiotics

The following macrolide antibiotics have been covered in this review: erythromycin and its related substances, azithromycin, clarithromycin, dirithromycin, roxithromycin, flurithromycin, josamycin, rokitamycin, kitasamycin, mycinamycin, mirosamycin, oleandomycin, rosaramicin, spiramycin and tylosin. The application of various thin-layer chromatography, paper chromatography, gas chromatography, high-performance liquid chromatography and capillary zone electrophoresis procedures for their …

Geographical distribution and accumulation features of organochlorine residues in fish in tropical Asia and Oceania

Concentrations of persistent organochlorine residues were determined in fish collected from several locations in eastern and southern Asia and Oceania to identifythe accumulation features of such residues in tropical aquatic organisms and to elucidate their distribution in tropical developing countries. DDT and its derivatives (DDTs) were the predominantly identified compounds …

Liquid chromatographic analysis of antibacterial drug residues in food products of animal origin

This paper reviews recent developments in the liquid chromatographic (LC) methods of analysis for the residues of antibiotics (aminoglycosides, chloramphenicol, sulfonamides, tetracyclines, macrolides, ?-lactams, etc.) in food products of animal origin. The review also covers clean-up procedures, such as, ultrafiltration, liquid-liquid partition, solid-phase extraction, immunoaffinity, and matrix solid-phase dispersion, for …

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